(bipyridine)(terpyridine)(4-iodophenylcyanamide)ruthenium(II) hexafluorophosphate

Base Information

Chemical Name:(bipyridine)(terpyridine)(4-iodophenylcyanamide)ruthenium(II) hexafluorophosphate
CAS No.:352020-07-6
Molecular Formula:C₃₂H₂₃IN₇Ru*F₆P
Molecular Weight:878.52
Hs Code.:

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Chemical Property of (bipyridine)(terpyridine)(4-iodophenylcyanamide)ruthenium(II) hexafluorophosphate

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Technology Process of (bipyridine)(terpyridine)(4-iodophenylcyanamide)ruthenium(II) hexafluorophosphate

There total 1 articles about (bipyridine)(terpyridine)(4-iodophenylcyanamide)ruthenium(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: ammonium hexafluorophosphate

: 26042-63-7
silver(I) hexafluorophosphate

: 83572-47-8
2,2'-bipyridine(2,2':6',2''-terpyridine)chlororuthenium(II) hexafluorophosphate

: 352020-08-7
N-(4-iodophenyl)cyanamide

: 352020-07-6
(bipyridine)(terpyridine)(4-iodophenylcyanamide)ruthenium(II) hexafluorophosphate

Guidance literature:: In acetone; byproducts: AgCl; mixt. of the Ru complex and AgPF6 refluxed with stirring for 4 h under Ar, a tenfold excess of ligand was added, soln. was stirred and refluxed for 4 h under Ar, then at room temp. overnight; AgCl was filtered off, solid NH4PF6 was added to the filtrate, soln. wasconcd., Et2O was added, ppt. was filtered, washed with Et2O, dried unde r vac., chromd., recrystd. from toluene and MeCN; elem. anal.;
DOI:10.1016/S0020-1693(01)00382-6