Technology Process of C22H22N4O2S
There total 4 articles about C22H22N4O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trichlorophosphate / acetonitrile / 1 h / 150 °C / Microwave irradiation
2: sodium 3,3′,3″-phosphinetriyltribenzenesulfonate tetrahydrate; palladium diacetate; caesium carbonate / acetonitrile; water / 0.08 h / 150 °C / Microwave irradiation
3: HATU; N-ethyl-N,N-diisopropylamine / dimethyl amine
With
sodium 3,3′,3″-phosphinetriyltribenzenesulfonate tetrahydrate; palladium diacetate; caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU; trichlorophosphate;
In
water; dimethyl amine; acetonitrile;
2: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2013.12.123
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trichlorophosphate / acetonitrile / 1 h / 150 °C / Microwave irradiation
2: sodium 3,3′,3″-phosphinetriyltribenzenesulfonate tetrahydrate; palladium diacetate; caesium carbonate / acetonitrile; water / 0.08 h / 150 °C / Microwave irradiation
3: HATU; N-ethyl-N,N-diisopropylamine / dimethyl amine
With
sodium 3,3′,3″-phosphinetriyltribenzenesulfonate tetrahydrate; palladium diacetate; caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU; trichlorophosphate;
In
water; dimethyl amine; acetonitrile;
2: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2013.12.123
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium 3,3′,3″-phosphinetriyltribenzenesulfonate tetrahydrate; palladium diacetate; caesium carbonate / acetonitrile; water / 0.08 h / 150 °C / Microwave irradiation
2: HATU; N-ethyl-N,N-diisopropylamine / dimethyl amine
With
sodium 3,3′,3″-phosphinetriyltribenzenesulfonate tetrahydrate; palladium diacetate; caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU;
In
water; dimethyl amine; acetonitrile;
1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2013.12.123