Technology Process of Bis-6-(10-mercaptodecyl)-bisubiquinone
There total 10 articles about Bis-6-(10-mercaptodecyl)-bisubiquinone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide; iodine;
In
ethyl acetate;
at 20 ℃;
for 0.5h;
DOI:10.1021/ja204014s
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium borohydride / methanol / 0.5 h / 0 °C
2: sodium hydroxide / ethanol; water / 0 - 20 °C
3: tetrahydrofuran / 4 h / Reflux; Inert atmosphere
4: ammonium cerium (IV) nitrate / water; acetonitrile / 0.83 h / 0 - 20 °C
5: potassium borohydride / methanol / 0.5 h / 0 °C / Inert atmosphere
6: hydrogenchloride / methanol; water / 3 h / 45 °C / Inert atmosphere
7: dihydrogen peroxide; iodine / ethyl acetate / 0.5 h / 20 °C
With
hydrogenchloride; ammonium cerium (IV) nitrate; potassium borohydride; dihydrogen peroxide; iodine; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; water; ethyl acetate; acetonitrile;
DOI:10.1021/ja204014s
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrahydrofuran / 4 h / Reflux; Inert atmosphere
2: ammonium cerium (IV) nitrate / water; acetonitrile / 0.83 h / 0 - 20 °C
3: potassium borohydride / methanol / 0.5 h / 0 °C / Inert atmosphere
4: hydrogenchloride / methanol; water / 3 h / 45 °C / Inert atmosphere
5: dihydrogen peroxide; iodine / ethyl acetate / 0.5 h / 20 °C
With
hydrogenchloride; ammonium cerium (IV) nitrate; potassium borohydride; dihydrogen peroxide; iodine;
In
tetrahydrofuran; methanol; water; ethyl acetate; acetonitrile;
DOI:10.1021/ja204014s
