2,3,4,5-tetramethoxy-6-(10-thioacetyldecyl)-toluene

Base Information

Chemical Name:2,3,4,5-tetramethoxy-6-(10-thioacetyldecyl)-toluene
CAS No.:1319741-66-6
Molecular Formula:C₂₃H₃₈O₅S
Molecular Weight:426.618
Hs Code.:

Synonyms:

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Chemical Property of 2,3,4,5-tetramethoxy-6-(10-thioacetyldecyl)-toluene

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Technology Process of 2,3,4,5-tetramethoxy-6-(10-thioacetyldecyl)-toluene

There total 6 articles about 2,3,4,5-tetramethoxy-6-(10-thioacetyldecyl)-toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 336184-90-8
C₁₉H₃₁BrO₄

: 1319741-66-6
2,3,4,5-tetramethoxy-6-(10-thioacetyldecyl)-toluene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol; water / 0 - 20 °C

2: tetrahydrofuran / 4 h / Reflux; Inert atmosphere

With sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/ja204014s

Reference yield:

: 81575-48-6
2-(10-bromodecyl)-5,6-dimethoxy-3-methylcyclohexa-2,5-diene-1,4-dione

: 1319741-66-6
2,3,4,5-tetramethoxy-6-(10-thioacetyldecyl)-toluene

Guidance literature:: Multi-step reaction with 3 steps

1: potassium borohydride / methanol / 0.5 h / 0 °C

2: sodium hydroxide / ethanol; water / 0 - 20 °C

3: tetrahydrofuran / 4 h / Reflux; Inert atmosphere

With potassium borohydride; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; water;
DOI:10.1021/ja204014s

Reference yield:

: 15949-84-5
11-bromoundecanoyl chloride

: 1319741-66-6
2,3,4,5-tetramethoxy-6-(10-thioacetyldecyl)-toluene

Guidance literature:: Multi-step reaction with 5 steps

1: dihydrogen peroxide / pyridine; diethyl ether / 1.75 h / 0 - 20 °C

2: acetic acid / 20 h / 100 °C

3: potassium borohydride / methanol / 0.5 h / 0 °C

4: sodium hydroxide / ethanol; water / 0 - 20 °C

5: tetrahydrofuran / 4 h / Reflux; Inert atmosphere

With potassium borohydride; dihydrogen peroxide; acetic acid; sodium hydroxide; In tetrahydrofuran; pyridine; methanol; diethyl ether; ethanol; water;
DOI:10.1021/ja204014s