6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside

Base Information

Chemical Name:6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside
CAS No.:852311-81-0
Molecular Formula:C₅₃H₈₀N₂O₁₆Si
Molecular Weight:1029.31
Hs Code.:

6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside

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Suppliers and Price of 6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside

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Chemical Property of 6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside

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Technology Process of 6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside

There total 10 articles about 6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852311-78-5
ethyl 2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

: 852311-80-9
6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(3,4-O-isopropylidene-α-L-fucopyranosyl)-β-D-glucopyranoside

: 6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-β-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside

: 852311-81-0
6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; tetrabutylammomium bromide; copper(ll) bromide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 96h;
DOI:10.1016/j.bmc.2005.02.009

Reference yield:

: 138343-54-1
ethyl 3,4-di-O-isopropylidene-1-thio-β-L-fucopyranoside

: 852311-81-0
6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / imidazole / dimethylformamide / 16 h / 20 °C

2: 291 mg / tetrabutylammonium bromide; copper(II) bromide; molecular sieves 4 Angstroem / CH₂Cl₂; dimethylformamide / 96 h / 20 °C

With 1H-imidazole; 4 A molecular sieve; tetrabutylammomium bromide; copper(ll) bromide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.02.009

Reference yield:

: 852311-78-5
ethyl 2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

: 852311-81-0
6-[N-(benzyloxycarbonylamino)hexyl]-2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-[3,4-O-isopropylidene-2-O-(2-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-L-fucopyranosyl)-α-L-fucopyranosyl]-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / tetrabutylammonium bromide; copper(II) bromide; molecular sieves 4 Angstroem / CH₂Cl₂; dimethylformamide / 48 h / 20 °C

2: 88 percent / tetrabutylammonium fluoride / tetrahydrofuran / 16 h / 20 °C

3: 291 mg / tetrabutylammonium bromide; copper(II) bromide; molecular sieves 4 Angstroem / CH₂Cl₂; dimethylformamide / 96 h / 20 °C

With 4 A molecular sieve; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; copper(ll) bromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.02.009