C₄₄H₆₇F₂N₃O₆Si

Base Information

Chemical Name:C₄₄H₆₇F₂N₃O₆Si
CAS No.:1345706-04-8
Molecular Formula:C₄₄H₆₇F₂N₃O₆Si
Molecular Weight:800.115
Hs Code.:

C<sub>44</sub>H<sub>67</sub>F<sub>2</sub>N<sub>3</sub>O<sub>6</sub>Si

Synonyms:

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Chemical Property of C₄₄H₆₇F₂N₃O₆Si

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Technology Process of C₄₄H₆₇F₂N₃O₆Si

There total 16 articles about C₄₄H₆₇F₂N₃O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 877078-49-4
(S)-4-benzyl-3-(3-(3,5-difluorophenyl)propanoyl)oxazolidin-2-one

: 1345706-04-8
C₄₄H₆₇F₂N₃O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 20 °C

2: 2,6-dimethylpyridine / dichloromethane

3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water

4: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 75 °C

5: 75 °C

6: palladium on activated charcoal; hydrogen / methanol

7: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide

With 4-methyl-morpholine; 2,6-dimethylpyridine; di-n-butylboryl trifluoromethanesulfonate; diphenyl phosphoryl azide; palladium on activated charcoal; HATU; hydrogen; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2011.06.109

Reference yield:

: 1345706-87-7
C₁₉H₂₇NO₃

: 1345706-04-8
C₄₄H₆₇F₂N₃O₆Si

Guidance literature:: Multi-step reaction with 4 steps

1: ozone / methanol

2: triethylsilane; trifluoroacetic acid / dichloromethane / 0 °C

3: lithium hydroxide / tetrahydrofuran / 20 °C

4: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide

With 4-methyl-morpholine; triethylsilane; HATU; ozone; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.06.109

Reference yield:

: 1345707-05-2
C₁₈H₂₅NO₃

: 1345706-04-8
C₄₄H₆₇F₂N₃O₆Si

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / tetrahydrofuran / 20 °C

2: 4-methyl-morpholine; HATU / N,N-dimethyl-formamide

With 4-methyl-morpholine; HATU; lithium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.06.109