C₂₇H₃₃N₃O₆S

Base Information

• Chemical Name: C₂₇H₃₃N₃O₆S
• CAS No.: 1584709-24-9
• Molecular Formula: C₂₇H₃₃N₃O₆S
• Molecular Weight: 527.642
• Mol file: 1584709-24-9.mol

Synonyms:

Chemical Property of C₂₇H₃₃N₃O₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₃₃N₃O₆S

There total 6 articles about C₂₇H₃₃N₃O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

((S)-methyl 3-(tert-Butoxycarbonyl)amino)-4-(4-(3-oxopropoxy)phenyl)butanoate (1426302-57-9) → C27H33N3O6S (1584709-24-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: magnesium sulfate monohydrate / dichloromethane / 1 h / 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / 20 °C / Inert atmosphere

With magnesium sulfate monohydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;

DOI:10.1021/jm500092w

Reference yield:

2-amino-4-methoxypyridine (10201-73-7) → C27H33N3O6S (1584709-24-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: magnesium sulfate monohydrate / dichloromethane / 1 h / 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / 20 °C / Inert atmosphere

With magnesium sulfate monohydrate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;

DOI:10.1021/jm500092w

Reference yield:

(S)-methyl 3-((tert-butoxycarbonyl)amino)-4-(4-(3-hydroxypropoxy)phenyl)butanoate (1426302-56-8) → C27H33N3O6S (1584709-24-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: Dess-Martin periodane / dichloromethane / 1.5 h / Inert atmosphere

2.1: magnesium sulfate monohydrate / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / 20 °C / Inert atmosphere

With magnesium sulfate monohydrate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;

DOI:10.1021/jm500092w

upstream raw materials:

((S)-methyl 3-(tert-Butoxycarbonyl)amino)-4-(4-(3-oxopropoxy)phenyl)butanoate

2-amino-4-methoxypyridine

(S)-N-(tert-butoxycarbonyl)tyrosine methyl ester

p-toluenesulfonyl chloride