1,2-diphenyl-9,12-diiodo-1,2-closo-dodecacarborane

Base Information

Chemical Name:1,2-diphenyl-9,12-diiodo-1,2-closo-dodecacarborane
CAS No.:634196-66-0
Molecular Formula:C₁₄H₁₈B₁₀I₂
Molecular Weight:548.216
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-diphenyl-9,12-diiodo-1,2-closo-dodecacarborane

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Technology Process of 1,2-diphenyl-9,12-diiodo-1,2-closo-dodecacarborane

There total 1 articles about 1,2-diphenyl-9,12-diiodo-1,2-closo-dodecacarborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.2%

: 17805-19-5
1,2-diphenyl-ortho-carborane

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 634196-66-0
1,2-diphenyl-9,12-diiodo-1,2-closo-dodecacarborane

Guidance literature:: With H₂SO₄; HNO₃; In acetic acid; N2, heated to 50°C, a mixture of mineral acids added dropwise over 30 min, stirred for 2 h; cooled, poured into H2O, solid dissolved (diethyl ether), dried (MgSO4),recrystd. (petroleum ether, -30°C); elem. anal.;
DOI:10.1016/S0277-5387(03)00103-7