Technology Process of 5-Decyl-2-(1,4,7,10,13,16-hexaoxa-cyclononadec-8-ylmethoxy)-benzoic acid methyl ester
There total 11 articles about 5-Decyl-2-(1,4,7,10,13,16-hexaoxa-cyclononadec-8-ylmethoxy)-benzoic acid methyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) potassium t-butoxide / 1.) THF, room temperature, 1 h; 2.) room temperature, 2 d, then reflux, 24 h
2: H2, p-toluenesulfonic acid / 10percent Pd on carbon / ethanol / 24 h / 760 Torr
3: 91 percent / pyridine / 4 °C / overnight
4: 1.) NaH / 1.) THF, room temperature, 1 h; 2.) reflux, 72 h
With
potassium tert-butylate; hydrogen; sodium hydride; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
pyridine; ethanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: H2, p-toluenesulfonic acid / 10percent Pd on carbon / ethanol / 24 h / 760 Torr
2: 91 percent / pyridine / 4 °C / overnight
3: 1.) NaH / 1.) THF, room temperature, 1 h; 2.) reflux, 72 h
With
hydrogen; sodium hydride; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
pyridine; ethanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) potassium t-butoxide / 1.) THF, room temperature, 1 h; 2.) room temperature, 2 d, then reflux, 24 h
2: H2, p-toluenesulfonic acid / 10percent Pd on carbon / ethanol / 24 h / 760 Torr
3: 91 percent / pyridine / 4 °C / overnight
4: 1.) NaH / 1.) THF, room temperature, 1 h; 2.) reflux, 72 h
With
potassium tert-butylate; hydrogen; sodium hydride; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
pyridine; ethanol;
