C₃₀H₂₂N₂O₄S

Base Information

Chemical Name:C₃₀H₂₂N₂O₄S
CAS No.:1266707-70-3
Molecular Formula:C₃₀H₂₂N₂O₄S
Molecular Weight:506.582
Hs Code.:

C<sub>30</sub>H<sub>22</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:

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Chemical Property of C₃₀H₂₂N₂O₄S

Chemical Property:

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Technology Process of C₃₀H₂₂N₂O₄S

There total 5 articles about C₃₀H₂₂N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 206768-50-5
5-((trimethylsilyl)ethynyl)thiophene-2-carbaldehyde

: 1266707-70-3
C₃₀H₂₂N₂O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / methanol / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20.5 h / 25 - 30 °C / Inert atmosphere

3: piperidine / acetonitrile / 4 h / Inert atmosphere; Reflux

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; acetonitrile; 2: Sonogashira coupling / 3: Knoevenagel condensation;
DOI:10.1039/c0nj00653j

Reference yield:

: 4701-17-1
5-bromo-2-thiophencarboxaldehyde

: 1266707-70-3
C₃₀H₂₂N₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

2: potassium carbonate / methanol / Inert atmosphere

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20.5 h / 25 - 30 °C / Inert atmosphere

4: piperidine / acetonitrile / 4 h / Inert atmosphere; Reflux

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; acetonitrile; 1: Sonagashira coupling / 3: Sonogashira coupling / 4: Knoevenagel condensation;
DOI:10.1039/c0nj00653j

Reference yield:

: 696-62-8
para-iodoanisole

: 1266707-70-3
C₃₀H₂₂N₂O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide / toluene / 100 °C / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20.5 h / 25 - 30 °C / Inert atmosphere

3: piperidine / acetonitrile / 4 h / Inert atmosphere; Reflux

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1,10-Phenanthroline; triethylamine; copper(l) chloride; potassium hydroxide; In tetrahydrofuran; toluene; acetonitrile; 1: Buchwald coupling / 2: Sonogashira coupling / 3: Knoevenagel condensation;
DOI:10.1039/c0nj00653j