Technology Process of C23H30ClNO3
There total 2 articles about C23H30ClNO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydrogencarbonate; sodium iodide / tetrahydrofuran; dimethyl sulfoxide / 12 h / Inert atmosphere; Reflux
2: methyllithium / diethyl ether / -90 °C / Inert atmosphere
With
methyllithium; sodium hydrogencarbonate; sodium iodide;
In
tetrahydrofuran; diethyl ether; dimethyl sulfoxide;
DOI:10.1002/adsc.201100497
- Guidance literature:
-
Multi-step reaction with 3 steps
1: chloro-trimethyl-silane / Inert atmosphere
2: sodium hydrogencarbonate; sodium iodide / tetrahydrofuran; dimethyl sulfoxide / 12 h / Inert atmosphere; Reflux
3: methyllithium / diethyl ether / -90 °C / Inert atmosphere
With
chloro-trimethyl-silane; methyllithium; sodium hydrogencarbonate; sodium iodide;
In
tetrahydrofuran; diethyl ether; dimethyl sulfoxide;
DOI:10.1002/adsc.201100497
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at -100 ℃;
for 6h;
Inert atmosphere;
DOI:10.1002/adsc.201100497