1--1-methylhydrazine

Base Information

• Chemical Name: 1--1-methylhydrazine
• CAS No.: 74763-72-7
• Molecular Formula: C₁₀H₁₄N₂O₂
• Molecular Weight: 194.233
• Mol file: 74763-72-7.mol

Synonyms:

Chemical Property of 1--1-methylhydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1--1-methylhydrazine

There total 2 articles about 1--1-methylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 4-N-methyl-N-nitrosoaminobenzoate (208176-48-1) → 1--1-methylhydrazine (74763-72-7)

Guidance literature:

With ethanol; acetic acid; zinc;

Reference yield:

→ 1--1-methylhydrazine (74763-72-7)

Guidance literature:

Aus Verb. 4e;

DOI:10.1021/ja01051a046

Reference yield: 33.0%

1--1-methylhydrazine (74763-72-7) → 1,4-Bis-(p-methylphenyl)-1,4-dimethyl-2-tetrazen (26190-49-8) + 1.4-Dimethyl-1-(4'-tolyl)-4-(p-carbaethoxyphenyl)-2-tetrazen (26190-53-4) + 1.4-Dimethyl-1.4-bis(4-carbaethoxyphenyl)-2-tetrazen (26190-51-2)

Guidance literature:

With lead dioxide; N-methyl-N-(4-tolyl)hydrazine;

DOI:10.1021/jo01310a036

upstream raw materials:

ethyl 4-N-methyl-N-nitrosoaminobenzoate

Downstream raw materials:

1,4-Bis-(p-methylphenyl)-1,4-dimethyl-2-tetrazen

1.4-Dimethyl-1-(4'-tolyl)-4-(p-carbaethoxyphenyl)-2-tetrazen

1.4-Dimethyl-1.4-bis(4-carbaethoxyphenyl)-2-tetrazen

C₂₀H₂₄N₂O₄