C₂₂H₄₀O₉P₂

Base Information

Chemical Name:C₂₂H₄₀O₉P₂
CAS No.:1370018-78-2
Molecular Formula:C₂₂H₄₀O₉P₂
Molecular Weight:510.502
Hs Code.:

C<sub>22</sub>H<sub>40</sub>O<sub>9</sub>P<sub>2</sub>

Synonyms:

Suppliers and Price of C₂₂H₄₀O₉P₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₂H₄₀O₉P₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₂H₄₀O₉P₂

There total 2 articles about C₂₂H₄₀O₉P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13071-59-5,17325-85-8,56552-80-8,4799-67-1
3-benzyloxypropan-1,2-diol

: 682-30-4
Diethyl vinylphosphonate

: 1370018-78-2
C₂₂H₄₀O₉P₂

Guidance literature:: With caesium carbonate; In tert-butyl alcohol; at 20 ℃; for 120h; Inert atmosphere;
DOI:10.1021/jm301893b

Reference yield:

: 15028-56-5
4-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxolane

: 1370018-78-2
C₂₂H₄₀O₉P₂

Guidance literature:: Multi-step reaction with 2 steps

1: Dowex (50X₈; 80 g) / methanol; water / 4 h / Reflux

2: caesium carbonate / tert-butyl alcohol / 120 h / 20 °C / Inert atmosphere

With caesium carbonate; In methanol; water; tert-butyl alcohol;
DOI:10.1021/jm301893b

Reference yield:

: 1370018-78-2
C₂₂H₄₀O₉P₂

: 1427428-95-2
C₅₆H₇₂N₈O₁₃P₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium 10% on activated carbon; palladium dichloride; hydrogenchloride / methanol; water / 20 °C

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / -30 - 20 °C / Inert atmosphere

3.1: trifluoroacetic acid; water

4.1: trimethylsilyl bromide; pyridine / acetonitrile / 20 °C / Inert atmosphere

4.2: 72 h / 60 - 70 °C / Inert atmosphere

With pyridine; hydrogenchloride; trimethylsilyl bromide; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; water; triphenylphosphine; trifluoroacetic acid; palladium dichloride; In tetrahydrofuran; methanol; water; acetonitrile; 2.1: |Mitsunobu Displacement;
DOI:10.1021/jm301893b