tris(trifluoromethyl)borane-dicyclohexylamine

Base Information

Chemical Name:tris(trifluoromethyl)borane-dicyclohexylamine
CAS No.:128354-00-7
Molecular Formula:C₁₅H₂₃BF₉N
Molecular Weight:399.151
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris(trifluoromethyl)borane-dicyclohexylamine

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Technology Process of tris(trifluoromethyl)borane-dicyclohexylamine

There total 1 articles about tris(trifluoromethyl)borane-dicyclohexylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 75-63-8
Bromotrifluoromethane

: 100384-01-8
(dicyclohexylamino)boron dichloride

: 128354-00-7
tris(trifluoromethyl)borane-dicyclohexylamine

Guidance literature:: With P(NEt₂)3; HCl; In dichloromethane; saturation of soln. of borane in dry CH2Cl2 with gaseous CF3Br at 0°C and dropwise addn. of P(NEt2)3 through which a stream of CF3Br was passed, stirring for 1 h at room temp.; solvent removal in vac., treating of viscous residue with conc. HCl, filtn. and recrystn. from CHCl3, elem. anal.;
DOI:10.1016/0022-328X(90)87281-H