1,1-Dichloro-N,N-dicyclohexylboranamine

Base Information

• Chemical Name: 1,1-Dichloro-N,N-dicyclohexylboranamine
• CAS No.: 100384-01-8
• Molecular Formula: C12H22BCl2N
• Molecular Weight: 262.03
• DSSTox Substance ID: DTXSID60571721
• Wikidata: Q82459883
• Mol file: 100384-01-8.mol

Synonyms:100384-01-8;1,1-Dichloro-N,N-dicyclohexylboranamine;N-cyclohexyl-N-dichloroboranylcyclohexanamine;DTXSID60571721

Chemical Property of 1,1-Dichloro-N,N-dicyclohexylboranamine

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 261.1222353
• Heavy Atom Count: 16
• Complexity: 183

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: B(N(C1CCCCC1)C2CCCCC2)(Cl)Cl

Technology Process of 1,1-Dichloro-N,N-dicyclohexylboranamine

There total 2 articles about 1,1-Dichloro-N,N-dicyclohexylboranamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

boron trichloride (10294-34-5) + N-cyclohexyl-cyclohexanamine (101-83-7) → (dicyclohexylamino)boron dichloride (100384-01-8)

Guidance literature:

DOI:10.1021/ja01530a010

Reference yield:

N-cyclohexyl-cyclohexanamine (101-83-7) → (dicyclohexylamino)boron dichloride (100384-01-8)

Guidance literature:

With boron trichloride;

DOI:10.1021/ja01530a010

Reference yield: 75.0%

(dicyclohexylamino)boron dichloride (100384-01-8) → (CH3)2BN(c-C6H11)(c-C6H11) (106474-35-5)

Guidance literature:

With methylmagnesium bromide; Grignard reaction;

DOI:10.1021/ja01530a010

upstream raw materials:

N-cyclohexyl-cyclohexanamine

boron trichloride

Downstream raw materials:

(CH₃)2BN(c-C₆H₁₁)(c-C₆H₁₁)

ClB{N(c-C₆H₁₁)2}{N(Si(CH₃)3)2}

tris(trifluoromethyl)borane-dicyclohexylamine

1,3-dichloro-1,3-bis(dicyclohexylamino)-1,3-diboroxane

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