C₂₄H₂₂O₃

Base Information

• Chemical Name: C₂₄H₂₂O₃
• CAS No.: 1327267-88-8
• Molecular Formula: C₂₄H₂₂O₃
• Molecular Weight: 358.437
• Mol file: 1327267-88-8.mol

Synonyms:

Chemical Property of C₂₄H₂₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₂O₃

There total 6 articles about C₂₄H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-benzofuran-1(3H)-one (87-41-2) → C24H22O3 (1327267-88-8)

Guidance literature:

Multi-step reaction with 6 steps

1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 20 °C

2: sodium hydride; sodium iodide / N,N-dimethyl-formamide

3: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C

4: sodium hydride / tetrahydrofuran / 16 h / 20 °C

5: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0.17 h / 60 °C

6: acetic acid / water / 16 h

With sodium tetrahydroborate; lithium aluminium tetrahydride; oxalyl dichloride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; sodium iodide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 3: Swern oxidation / 4: Claisen Schmidt condensation;

DOI:10.1055/s-0030-1260564

Reference yield:

C24H24O4 → C24H22O3 (1327267-88-8)

Guidance literature:

With acetic acid; In water; for 16h;

DOI:10.1055/s-0030-1260564

Reference yield:

2-{[(4-methoxybenzyl)oxy]methyl}benzaldehyde → C24H22O3 (1327267-88-8)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 16 h / 20 °C

2: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0.17 h / 60 °C

3: acetic acid / water / 16 h

With sodium tetrahydroborate; sodium hydride; acetic acid; In tetrahydrofuran; ethanol; water; 1: Claisen Schmidt condensation;

DOI:10.1055/s-0030-1260564

upstream raw materials:

2-benzofuran-1(3H)-one

(2-{[(4-methoxybenzyl)oxy]methyl}phenyl)methanol

phthalyl alcohol

Downstream raw materials:

2-o-tolyl-chroman

C₂₄H₂₄O₃