ferrocenyl(phenyl)dichlorogermane

Base Information

Chemical Name:ferrocenyl(phenyl)dichlorogermane
CAS No.:403817-43-6
Molecular Formula:C₁₆H₁₄Cl₂FeGe
Molecular Weight:405.63
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ferrocenyl(phenyl)dichlorogermane

Chemical Property:

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Technology Process of ferrocenyl(phenyl)dichlorogermane

There total 1 articles about ferrocenyl(phenyl)dichlorogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 403817-49-2
Fe(C₅H₄)2C₆H₅GeCl

: 403817-43-6
ferrocenyl(phenyl)dichlorogermane

Guidance literature:: In diethyl ether; hexane; to soln. of Fe-complex in hexane was added dropwise at room temp. HCl inether, stirred for 15 min under Ar; filtered, solvent was removed in vacuo; elem. anal.;
DOI:10.1016/S0022-328X(01)00962-7

Reference yield: 69.0%

: 102-54-5,55404-68-7
ferrocene

: 403817-43-6
ferrocenyl(phenyl)dichlorogermane

: 403817-45-8
poly-ferrocenylenephenylferrocenylgermylene

Guidance literature:: With n-BuLi; TMEDA; In diethyl ether; hexane; to soln. of ferrocene, TMEDA in hexane was added n-BuLi, stirred for 18 h, washed with hexane, ether was added, stirred at -78°C, Fe-complex in ether was added, warmed to room temp., stirred overnight under Ar; solvent was removed in vacuo, washed with hexane, dissolved in toluene and THF, filtered, solvent was removed under vac., recrystd. from THF; elem. anal.;
DOI:10.1016/S0022-328X(01)00962-7

Reference yield:

: 403817-43-6
ferrocenyl(phenyl)dichlorogermane

: 7732-18-5
water

: cis-1,3,5-triphenyl-1,3,5-triferrocenylcyclotrigermanoxane

: trans-1,3,5-triphenyl-1,3,5-triferrocenylcyclotrigermanoxane

Guidance literature:: With Et₃N; In diethyl ether; acetone; byproducts: Et3NHCl; under N2; Et2O soln. of Fe complex added dropwise to soln. of H2O and Et3N in ether-acetone; stirred for 1 h; concd.; hexane added; filtered; solvent removed under vac.; cis and trans isomers (1:4) obtained; recrystd. from CH2Cl2-hexane (cis); mixt. of isomers in 95% EtOH (4 drops NaOH) refluxed (2 h); cooled to -15°C overnight; filtrate dried under vac. (trans); elem. anal.;
DOI:10.1021/om020788p