4-benzyl-1-benzyloxycarbonyl-S-methyl-isothiosemicarbazide hydrogen iodide

Base Information

Chemical Name:4-benzyl-1-benzyloxycarbonyl-S-methyl-isothiosemicarbazide hydrogen iodide
CAS No.:88104-49-8
Molecular Formula:C₂₃H₂₃N₃O₂S*HI
Molecular Weight:533.433
Hs Code.:

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Chemical Property of 4-benzyl-1-benzyloxycarbonyl-S-methyl-isothiosemicarbazide hydrogen iodide

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Technology Process of 4-benzyl-1-benzyloxycarbonyl-S-methyl-isothiosemicarbazide hydrogen iodide

There total 4 articles about 4-benzyl-1-benzyloxycarbonyl-S-methyl-isothiosemicarbazide hydrogen iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 88104-48-7
4-benzyl-1-benzyloxycarbonyl-2-phenyl-thiosemicarbazide

: 74-88-4
methyl iodide

: 88104-49-8
4-benzyl-1-benzyloxycarbonyl-S-methyl-isothiosemicarbazide hydrogen iodide

Guidance literature:: In acetone; for 20h;
DOI:10.1016/S0040-4020(01)92153-2

Reference yield:

: 40887-05-6
N¹-benzyloxycarbonyl-N²-phenylhydrazide

: 88104-49-8
4-benzyl-1-benzyloxycarbonyl-S-methyl-isothiosemicarbazide hydrogen iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / methylcyclohexane / 24 h / Heating

2: 94 percent / acetone / 20 h

In methyl cyclohexane; acetone;
DOI:10.1016/S0040-4020(01)92153-2

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 88104-49-8
4-benzyl-1-benzyloxycarbonyl-S-methyl-isothiosemicarbazide hydrogen iodide

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 0.33 h / 0 - 10 °C

2: 81 percent / methylcyclohexane / 24 h / Heating

3: 94 percent / acetone / 20 h

In diethyl ether; methyl cyclohexane; acetone;
DOI:10.1016/S0040-4020(01)92153-2