η(3)-(9-fluorenylidene)-η(3)-(1-(3-allyl)indenylidene)methylphenylsilane zirconium dichloride

Base Information

• Chemical Name: η(3)-(9-fluorenylidene)-η(3)-(1-(3-allyl)indenylidene)methylphenylsilane zirconium dichloride
• CAS No.: 212199-96-7
• Molecular Formula: C₃₂H₂₆Cl₂SiZr
• Molecular Weight: 600.774

Synonyms:

Chemical Property of η(3)-(9-fluorenylidene)-η(3)-(1-(3-allyl)indenylidene)methylphenylsilane zirconium dichloride

Chemical Property:

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Technology Process of η(3)-(9-fluorenylidene)-η(3)-(1-(3-allyl)indenylidene)methylphenylsilane zirconium dichloride

There total 1 articles about η(3)-(9-fluorenylidene)-η(3)-(1-(3-allyl)indenylidene)methylphenylsilane zirconium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-fluorenyl-1-(3-allyl)indenylmethylphenylsilane + zirconium(IV) chloride (10026-11-6) → η(3)-(9-fluorenylidene)-η(3)-(1-(3-allyl)indenylidene)methylphenylsilane zirconium dichloride (212199-96-7)

Guidance literature:

With n-butyllithium; In diethyl ether; hexane; byproducts: LiCl; stirring ligand (in Et2O) with 2 equiv. of BuLi (in hexane, room temp., 8 h), addn. of 1 equiv. of ZrCl4, stirring overnight; filtration off of LiCl; or evapn., dissoln. in CH2Cl2 or CH2Cl2/PhMe, evapn.; method not specified, depending on soly. of product in reaction solvent;

DOI:10.1016/S0022-328X(98)00538-5

upstream raw materials:

zirconium(IV) chloride

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