Technology Process of C35H26BrNO3
There total 8 articles about C35H26BrNO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: copper; potassium carbonate / nitrobenzene / 6 h / Inert atmosphere; Reflux
2: sodium hydroxide / ethanol / 20 °C
3: potassium hydroxide / ethanol; dichloromethane / 6 h / Reflux
4: potassium hydroxide / water; acetone / 20 °C
5: acetic acid; hydrogenchloride / water / Reflux
With
hydrogenchloride; copper; potassium carbonate; acetic acid; potassium hydroxide; sodium hydroxide;
In
ethanol; dichloromethane; water; nitrobenzene; acetone;
1: |Ullmann Condensation / 2: |Aldol Condensation / 3: |Michael Addition;
DOI:10.1002/cmdc.201400007
- Guidance literature:
-
Multi-step reaction with 5 steps
1: copper; potassium carbonate / nitrobenzene / 6 h / Inert atmosphere; Reflux
2: sodium hydroxide / ethanol / 20 °C
3: potassium hydroxide / ethanol; dichloromethane / 6 h / Reflux
4: potassium hydroxide / water; acetone / 20 °C
5: acetic acid; hydrogenchloride / water / Reflux
With
hydrogenchloride; copper; potassium carbonate; acetic acid; potassium hydroxide; sodium hydroxide;
In
ethanol; dichloromethane; water; nitrobenzene; acetone;
1: |Ullmann Condensation / 2: |Aldol Condensation / 3: |Michael Addition;
DOI:10.1002/cmdc.201400007
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / ethanol / 20 °C
2: potassium hydroxide / ethanol; dichloromethane / 6 h / Reflux
3: potassium hydroxide / water; acetone / 20 °C
4: acetic acid; hydrogenchloride / water / Reflux
With
hydrogenchloride; acetic acid; potassium hydroxide; sodium hydroxide;
In
ethanol; dichloromethane; water; acetone;
1: |Aldol Condensation / 2: |Michael Addition;
DOI:10.1002/cmdc.201400007