9-(2-Phenylethyl)-9H-fluorene

Base Information

Chemical Name:9-(2-Phenylethyl)-9H-fluorene
CAS No.:10423-31-1
Molecular Formula:C21H18
Molecular Weight:270.374
Hs Code.:
DSSTox Substance ID:DTXSID60488926
Nikkaji Number:J1.287.651C
Wikidata:Q82331913

Synonyms:9-(2-PHENYLETHYL)-9H-FLUORENE;10423-31-1;9-(2-Phenylethyl)fluorene;DTXSID60488926

Suppliers and Price of 9-(2-Phenylethyl)-9H-fluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 9-(2-Phenylethyl)-9H-fluorene

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:270.140850574
Heavy Atom Count:21
Complexity:305

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CCC2C3=CC=CC=C3C4=CC=CC=C24

Technology Process of 9-(2-Phenylethyl)-9H-fluorene

There total 5 articles about 9-(2-Phenylethyl)-9H-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 13029-09-9
2,2'-dibromobiphenyl

: 1379610-52-2
4,4,5,5‐tetramethyl‐2‐[5‐phenyl‐1‐(4,4,5,5‐tetramethyl‐1,3,2‐dioxaborolan‐2‐yl)propyl]‐1,3,2‐dioxaborolane

: 10423-31-1
9-phenethyl-9H-fluorene

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; sodium hydroxide; In 1,4-dioxane; water; at 25 ℃; for 48h; Reagent/catalyst; Temperature; Inert atmosphere;
DOI:10.1021/acs.joc.5b01100

Reference yield:

: 86-73-7
9H-fluorene

: 103-63-9
1-phenyl-2-bromoethane

: 10423-31-1
9-phenethyl-9H-fluorene

Guidance literature:: Multistep reaction; (i) PhLi, (ii) /BRN= 507487/;
DOI:10.1039/j39660001810

Reference yield:

: 61124-61-6
3-phenylpropanal p-tosylhydrazone

: 10423-31-1
9-phenethyl-9H-fluorene

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / toluene; mineral oil / 1 h / 20 °C / Inert atmosphere

1.2: 12 h / 110 °C

2.1: bis(tri-t-butylphosphine)palladium⁽⁰⁾; sodium hydroxide / water; 1,4-dioxane / 48 h / 25 °C / Inert atmosphere

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; sodium hydride; sodium hydroxide; In 1,4-dioxane; water; toluene; mineral oil;
DOI:10.1021/acs.joc.5b01100