Pd(Cl)(P(C₂H₅)3)2(C(Cl)PC₆H₂(C(CH₃)3)3)

Base Information

Chemical Name:Pd(Cl)(P(C₂H₅)3)2(C(Cl)PC₆H₂(C(CH₃)3)3)
CAS No.:156955-26-9
Molecular Formula:C₃₁H₅₉Cl₂P₃Pd
Molecular Weight:702.057
Hs Code.:

Pd(Cl)(P(C<sub>2</sub>H<sub>5</sub>)3)2(C(Cl)PC<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)3)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pd(Cl)(P(C₂H₅)3)2(C(Cl)PC₆H₂(C(CH₃)3)3)

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Technology Process of Pd(Cl)(P(C₂H₅)3)2(C(Cl)PC₆H₂(C(CH₃)3)3)

There total 1 articles about Pd(Cl)(P(C₂H₅)3)2(C(Cl)PC₆H₂(C(CH₃)3)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 52230-29-2
tetrakis(triethylphosphine)palladium

: 100281-24-1
2,2-dichloro-1-(2,4,6-tri-tert-butylphenyl)-1-phosphaethene

: 156955-26-9
Pd(Cl)(P(C₂H₅)3)2(C(Cl)PC₆H₂(C(CH₃)3)3)

Guidance literature:: In benzene; (Ar); phosphaalkene is added to Pt-compd., soln. is stirred at room temp. for 1 h; solvent is evapd. under vacuum, residue is extd. with hexanes and filtered by cannula, concn. under vacuum, crystn. at -78°C, elem. anal.;

Reference yield: 72.0%

: 156955-26-9
Pd(Cl)(P(C₂H₅)3)2(C(Cl)PC₆H₂(C(CH₃)3)3)

: 33937-26-7
tetrakis(triethylphosphine)platinum⁽⁰⁾

: 145637-60-1
Pd(Cl)(P(C₂H₅)3)2(C₆H₂(C(CH₃)3)3)

: Cl(Et3P)2Pt(μ-η(1),η(2)-CP)Pt(PEt3)2

Guidance literature:: In benzene; (Ar, Schlenk technique); soln. of Pt-complex is added to Pt(PEt3)4, mixt. is stirred for 12 h at room temp.; solvent is evapd. to dryness under vacuum, residue is extd. with hexaneand filtered by cannula, volume is reduced, crystn. at -78°C after 2-3 d (Pd-compd. is filtered off), volume is reduced under vacuum, crystn. at -78°C (2 weeks);

Reference yield: 36.0%

: 156955-26-9
Pd(Cl)(P(C₂H₅)3)2(C(Cl)PC₆H₂(C(CH₃)3)3)

: 28425-04-9
trans-dichlorobis(triethylphosphine)palladium(II)

Guidance literature:: In dichloromethane; byproducts: PC(C6H2(C(CH3)3)3); (Ar); complex is stirred at room temp. for 24 h; soln. is evapd. to dryness, residue is extd. with hexanes and filtered (Celite), column chromy. (silica, hexanes);