ethyl 4-benzoate

Base Information

Chemical Name:ethyl 4-benzoate
CAS No.:170799-72-1
Molecular Formula:C₁₂H₁₆INO₂
Molecular Weight:333.169
Hs Code.:

ethyl 4-<N-(2-iodoethyl)-N-methylamino>benzoate

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 4-benzoate

Chemical Property:

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Technology Process of ethyl 4-benzoate

There total 6 articles about ethyl 4-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 4-[(2-Methanesulfonyloxy-ethyl)-methyl-amino]-benzoic acid ethyl ester

: 170799-72-1
ethyl 4-benzoate

Guidance literature:: With sodium iodide;
DOI:10.1248/cpb.43.829

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 170799-72-1
ethyl 4-benzoate

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / N,N-diisopropylethylamine / dimethylformamide / 24 h / 70 °C

2: 63 percent / NaHCO₃ / 1 h / 90 °C

3: 55 percent / 1N NaOH / ethanol

4: 95 percent / NaBH₄

5: Et₃N

6: 93 percent / NaI

With sodium hydroxide; sodium tetrahydroborate; sodium hydrogencarbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.43.829

Reference yield:

: 149325-28-0
ethyl N-(4-ethoxycarbonylphenyl)-N-methylaminoacetate

: 170799-72-1
ethyl 4-benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / 1N NaOH / ethanol

2: 95 percent / NaBH₄

3: Et₃N

4: 93 percent / NaI

With sodium hydroxide; sodium tetrahydroborate; triethylamine; sodium iodide; In ethanol;
DOI:10.1248/cpb.43.829