C₃₄H₅₄N₂O₅Si₂

Base Information

Chemical Name:C₃₄H₅₄N₂O₅Si₂
CAS No.:1567326-75-3
Molecular Formula:C₃₄H₅₄N₂O₅Si₂
Molecular Weight:626.984
Hs Code.:

C<sub>34</sub>H<sub>54</sub>N<sub>2</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₃₄H₅₄N₂O₅Si₂

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Technology Process of C₃₄H₅₄N₂O₅Si₂

There total 16 articles about C₃₄H₅₄N₂O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 530-26-7
D-Mannose

: 1567326-75-3
C₃₄H₅₄N₂O₅Si₂

Guidance literature:: Multi-step reaction with 16 steps

1.1: iodine / 16 h / 20 °C

2.1: sodium cyanide / water / 12 h / 50 °C

2.2: 12 h / 20 °C

3.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

3.2: 20 h / 20 °C

4.1: acetic acid / water / 3.5 h / 50 °C

5.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

6.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

7.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

8.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

9.1: tetrahydrofuran; methanol / 2 h / 20 °C

10.1: potassium carbonate / N,N-dimethyl-formamide

11.1: acetic acid; methanol

12.1: toluene-4-sulfonic acid; trimethyl orthoformate / methanol / 75 °C

13.1: dichloromethane

14.1: toluene-4-sulfonic acid; methanol

15.1: N-ethyl-N,N-diisopropylamine

16.1: 1,1'-Thiocarbonyldiimidazole; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene

With pyridine; methanol; dmap; sodium cyanide; 2,2'-azobis(isobutyronitrile); trifluoromethylsulfonic anhydride; iodine; tri-n-butyl-tin hydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 1,1'-Thiocarbonyldiimidazole; triethyl phosphite; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 7757-38-2,14131-84-1,23262-78-4,27108-13-0,33823-04-0,34685-42-2,57819-52-0,78039-08-4,78039-12-0,78964-16-6,94842-76-9,149342-31-4
2,3:5,6-di-O-isopropylidene-D-mannofuranose

: 1567326-75-3
C₃₄H₅₄N₂O₅Si₂

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium cyanide / water / 12 h / 50 °C

1.2: 12 h / 20 °C

2.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

2.2: 20 h / 20 °C

3.1: acetic acid / water / 3.5 h / 50 °C

4.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

6.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

7.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

8.1: tetrahydrofuran; methanol / 2 h / 20 °C

9.1: potassium carbonate / N,N-dimethyl-formamide

10.1: acetic acid; methanol

11.1: toluene-4-sulfonic acid; trimethyl orthoformate / methanol / 75 °C

12.1: dichloromethane

13.1: toluene-4-sulfonic acid; methanol

14.1: N-ethyl-N,N-diisopropylamine

15.1: 1,1'-Thiocarbonyldiimidazole; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene

With pyridine; methanol; dmap; sodium cyanide; 2,2'-azobis(isobutyronitrile); trifluoromethylsulfonic anhydride; tri-n-butyl-tin hydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 1,1'-Thiocarbonyldiimidazole; triethyl phosphite; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 137126-24-0
(3aR,4R,7S,7aR)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-7-hydroxy-2,2-dimethyltetrahydro-[1,3]-dioxolo-[4,5-c]-pyran-6-one

: 1567326-75-3
C₃₄H₅₄N₂O₅Si₂

Guidance literature:: Multi-step reaction with 14 steps

1.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

1.2: 20 h / 20 °C

2.1: acetic acid / water / 3.5 h / 50 °C

3.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

4.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

5.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

6.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

7.1: tetrahydrofuran; methanol / 2 h / 20 °C

8.1: potassium carbonate / N,N-dimethyl-formamide

9.1: acetic acid; methanol

10.1: toluene-4-sulfonic acid; trimethyl orthoformate / methanol / 75 °C

11.1: dichloromethane

12.1: toluene-4-sulfonic acid; methanol

13.1: N-ethyl-N,N-diisopropylamine

14.1: 1,1'-Thiocarbonyldiimidazole; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene

With pyridine; methanol; dmap; 2,2'-azobis(isobutyronitrile); trifluoromethylsulfonic anhydride; tri-n-butyl-tin hydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 1,1'-Thiocarbonyldiimidazole; triethyl phosphite; trimethyl orthoformate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;