1-(3-bromopropyl)-1H-4-imidazolecarbaldehyde

Base Information

• Chemical Name: 1-(3-bromopropyl)-1H-4-imidazolecarbaldehyde
• CAS No.: 199191-93-0
• Molecular Formula: C₇H₉BrN₂O
• Molecular Weight: 217.065

Synonyms:

Chemical Property of 1-(3-bromopropyl)-1H-4-imidazolecarbaldehyde

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

1-(3-bromopropyl)-1H-Imidazole-4-carboxaldehyde 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3-bromopropyl)-1H-4-imidazolecarbaldehyde

There total 1 articles about 1-(3-bromopropyl)-1H-4-imidazolecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

4(5)formylimidazole (3034-50-2) + 1,3-dibromo-propane (109-64-8) → 1-(3-bromopropyl)-1H-4-imidazolecarbaldehyde (199191-93-0)

Guidance literature:

With sodium hydride; In tetrahydrofuran;

DOI:10.1016/S0040-4039(97)10052-1

Reference yield: 42.0%

1-(3-bromopropyl)-1H-4-imidazolecarbaldehyde (199191-93-0) → 1-n-Propyl-1H-imidazole-4-carboxaldehyde (199192-04-6) + 6,7-dihydro-5H-pyrrolo<1,2-c>imidazole-1-carbaldehyde

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In acetonitrile; for 5h; Heating;

DOI:10.1016/S0040-4039(97)10052-1

Reference yield: 41.0%

diphenyl diselenide (1666-13-3) + 1-(3-bromopropyl)-1H-4-imidazolecarbaldehyde (199191-93-0) → <1-<3-(phenylselanyl)propyl>-1H-4-imidazolyl>methanol

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 16h; Ambient temperature;

DOI:10.1016/S0040-4020(99)00419-6

upstream raw materials:

4⁽⁵⁾formylimidazole

1,3-dibromo-propane

Downstream raw materials:

1-n-Propyl-1H-imidazole-4-carboxaldehyde

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