Me₃Si(Me₃Ge)(Ph₃Sn)CH

Base Information

Chemical Name:Me₃Si(Me₃Ge)(Ph₃Sn)CH
CAS No.:226726-97-2
Molecular Formula:C₂₅H₃₄GeSiSn
Molecular Weight:553.93
Hs Code.:

Me<sub>3</sub>Si(Me<sub>3</sub>Ge)(Ph<sub>3</sub>Sn)CH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Me₃Si(Me₃Ge)(Ph₃Sn)CH

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Technology Process of Me₃Si(Me₃Ge)(Ph₃Sn)CH

There total 1 articles about Me₃Si(Me₃Ge)(Ph₃Sn)CH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 2290-62-2
trimethylgermyltrimethylsilylmethane

: 639-58-7
triphenyltin chloride

: 226726-97-2
Me₃Si(Me₃Ge)(Ph₃Sn)CH

Guidance literature:: With HMPA; t-butyllithium; In tetrahydrofuran; pentane; byproducts: LiCl; THF soln. Me3Si(Me3Ge)CH2 and HMPA at -78°C was treated with soln. t-BuLi in penane and stirred for 1 h, soln. Ph3SnCl was added slowly at -78°C, soln. was stirred and allowed to warm slowly to room temp.; react. mixt. was treated with hexane, washed with aq. NH4Cl soln., driedover MgSO4 overnight and filtered, solvent was removed, residue was rec rystd. from CH2Cl2-hexane;
DOI:10.1016/S0022-328X(03)00718-6