benzhydryl (phenyl) chromium tricarbonyl sufone

Base Information

Chemical Name:benzhydryl (phenyl) chromium tricarbonyl sufone
CAS No.:259145-10-3
Molecular Formula:C₂₂H₁₆CrO₅S
Molecular Weight:444.428
Hs Code.:

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Chemical Property of benzhydryl (phenyl) chromium tricarbonyl sufone

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Technology Process of benzhydryl (phenyl) chromium tricarbonyl sufone

There total 2 articles about benzhydryl (phenyl) chromium tricarbonyl sufone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: (2S,S(S))-2-hydroxy-1,1-dipphenylpropyl(benzene) chromiumtricarbonyl sufinate

: 677-22-5
tert-butylmagnesium chloride

: 259145-10-3
benzhydryl (phenyl) chromium tricarbonyl sufone

Guidance literature:: In tetrahydrofuran; N2; Cr-compd. soln. addn. to t-BuMgBr at room temp., stirring 14 h, quenching by satd. aq. NH4Cl addn., extn. (EtOAc), filtration (MgSO4/silica plug), solvent evapn.; crystn. (hexane/DCM 2:1); elem. anal.;
DOI:10.1039/a907590i

Reference yield: 9.0%

: (2S,S(S))-2-hydroxy-1,1-dipphenylpropyl(benzene) chromiumtricarbonyl sufinate

: (2S,S(S))-1-hydroxy-1,1-dipphenylpropan-yl(benzene) chromium tricarbonyl sufinate

: 159508-93-7
(S(S))-[(tert-butylsulfinyl)benzene] chromium tricarbonyl

: 259145-10-3
benzhydryl (phenyl) chromium tricarbonyl sufone

Guidance literature:: In tetrahydrofuran; N2; BuMgCl addn. dropwise to Cr-compds. soln. at room temp., stirring 45min, quenching by satd. aq. NH4Cl addn., extn. (EtOAc), filtration (MgS O4/silica plug), solvent evapn.; column chromy. (silica gel, petrol/EtOAc 1.5:1); (1)H NMR;
DOI:10.1039/a907590i