N-((3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)carbamoyl)-2-(2,4-dichlorophenoxy) acetamide

Base Information

Chemical Name:N-((3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)carbamoyl)-2-(2,4-dichlorophenoxy) acetamide
CAS No.:1591971-37-7
Molecular Formula:C₂₁H₉Cl₄F₆N₅O₄S
Molecular Weight:683.202
Hs Code.:

N-((3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)carbamoyl)-2-(2,4-dichlorophenoxy) acetamide

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Chemical Property of N-((3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)carbamoyl)-2-(2,4-dichlorophenoxy) acetamide

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Technology Process of N-((3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)carbamoyl)-2-(2,4-dichlorophenoxy) acetamide

There total 4 articles about N-((3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)carbamoyl)-2-(2,4-dichlorophenoxy) acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 5843-44-7
2-(2,4-dichlorophenoxy)acetyl isocyanate

: 120068-37-3
fipronil

: 1591971-37-7
N-((3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)carbamoyl)-2-(2,4-dichlorophenoxy) acetamide

Guidance literature:: In diethyl ether; at 0 - 20 ℃;
DOI:10.1021/jf405512e

Reference yield:

: 94-75-7,89300-30-1
2,4-Dichlorophenoxyacetic acid

: 1591971-37-7
N-((3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)carbamoyl)-2-(2,4-dichlorophenoxy) acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride

2: ammonium hydroxide

3: 1,2-dichloro-ethane

4: diethyl ether / 0 - 20 °C

With ammonium hydroxide; thionyl chloride; In diethyl ether; 1,2-dichloro-ethane;
DOI:10.1021/jf405512e

Reference yield:

: 774-74-3
2-(2,4-dichlorophenoxy)acetyl chloride

: 1591971-37-7
N-((3-cyano-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazol-5-yl)carbamoyl)-2-(2,4-dichlorophenoxy) acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium hydroxide

2: 1,2-dichloro-ethane

3: diethyl ether / 0 - 20 °C

With ammonium hydroxide; In diethyl ether; 1,2-dichloro-ethane;
DOI:10.1021/jf405512e