6-deoxy-6-fluoro-α-D-glucopyranosyl

Base Information

Chemical Name:6-deoxy-6-fluoro-α-D-glucopyranosyl
CAS No.:109923-27-5
Molecular Formula:C₆H₁₂FO₈P*2C₆H₁₃N
Molecular Weight:460.48
Hs Code.:

6-deoxy-6-fluoro-α-D-glucopyranosyl <bis(cyclohexylammonium) phosphate>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-deoxy-6-fluoro-α-D-glucopyranosyl

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 6-deoxy-6-fluoro-α-D-glucopyranosyl

There total 2 articles about 6-deoxy-6-fluoro-α-D-glucopyranosyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13100-46-4
1,2,3,4-tetra-O-acetyl-β-D-glucopyranose

: 109923-27-5
6-deoxy-6-fluoro-α-D-glucopyranosyl

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / diethylaminosulfur trifluoride, 2,4,6-trimethylpyridine / CH₂Cl₂ / 1) -20 deg C, 15 min, 2) RT, 24 h

2: 1) phosphoric acid, 2) Dowex 50W-X₈(1+)> / 1.) 55 deg C, 2.5 h

With 2,4,6-trimethyl-pyridine; diethylamino-sulfur trifluoride; phosphoric acid; Dowex 50W-X8; In dichloromethane;
DOI:10.1016/S0008-6215(00)90028-4

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 33557-29-8,674782-58-2
1,2,3,4-tetra-O-acetyl-6-deoxy-6-fluoro-β-D-glucopyranose

: 109923-27-5
6-deoxy-6-fluoro-α-D-glucopyranosyl

Guidance literature:: With phosphoric acid; Dowex 50W-X8; Yield given. Multistep reaction; 1.) 55 deg C, 2.5 h;
DOI:10.1016/S0008-6215(00)90028-4