2,3-Bis-(2,4,6-tri-tert-butyl-phenyl)-thiadiarsirane

Base Information

• Chemical Name: 2,3-Bis-(2,4,6-tri-tert-butyl-phenyl)-thiadiarsirane
• CAS No.: 120611-01-0
• Molecular Formula: C₃₆H₅₈As₂S
• Molecular Weight: 672.766
• Mol file: 120611-01-0.mol

Synonyms:

Chemical Property of 2,3-Bis-(2,4,6-tri-tert-butyl-phenyl)-thiadiarsirane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-Bis-(2,4,6-tri-tert-butyl-phenyl)-thiadiarsirane

There total 2 articles about 2,3-Bis-(2,4,6-tri-tert-butyl-phenyl)-thiadiarsirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

bis(2,4,6-tri-tert-butylphenyl)diarsene (120611-00-9) → 2,3-Bis-(2,4,6-tri-tert-butyl-phenyl)-thiadiarsirane (120611-01-0)

Guidance literature:

With sulfur; In benzene; for 0.5h; Heating;

Reference yield:

dichloro(2,4,6-tri-tert-butylphenyl)arsane (117184-75-5) → 2,3-Bis-(2,4,6-tri-tert-butyl-phenyl)-thiadiarsirane (120611-01-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 61 percent / Mg / tetrahydrofuran / 2 h / 0 °C

2: 63 percent / sulfur / benzene / 0.5 h / Heating

With sulfur; magnesium; In tetrahydrofuran; benzene;

upstream raw materials:

bis(2,4,6-tri-tert-butylphenyl)diarsene

dichloro(2,4,6-tri-tert-butylphenyl)arsane