2,10-dimethyl-6-phenyl-2,6,10-triphosphaundecane

Base Information

Chemical Name:2,10-dimethyl-6-phenyl-2,6,10-triphosphaundecane
CAS No.:79394-74-4
Molecular Formula:C₁₆H₂₉P₃
Molecular Weight:314.328
Hs Code.:

Synonyms:

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Chemical Property of 2,10-dimethyl-6-phenyl-2,6,10-triphosphaundecane

Chemical Property:

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Technology Process of 2,10-dimethyl-6-phenyl-2,6,10-triphosphaundecane

There total 2 articles about 2,10-dimethyl-6-phenyl-2,6,10-triphosphaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26681-86-7
Allyl-dimethyl-phosphin

: 638-21-1
phenylphosphane

: 79394-74-4
2,10-dimethyl-6-phenyl-2,6,10-triphosphaundecane

Guidance literature:: With 2,2'-azobis(isobutyronitrile); at 110 ℃; for 2h;

Reference yield:

: 79345-74-7
6-phenyl-2,6,10-triphosphaundecane

: 74-88-4
methyl iodide

: 79394-74-4
2,10-dimethyl-6-phenyl-2,6,10-triphosphaundecane

Guidance literature:: With methyllithium; Yield given. Multistep reaction; 1) THF, diethyl ether, 2) THF, diethyl ether, -25 deg C to 20 deg C;

Reference yield: 78.0%

: nickel(II) bromide trihydrate

: 79394-74-4
2,10-dimethyl-6-phenyl-2,6,10-triphosphaundecane

: 79351-81-8
dibromo(2,10-dimethyl-6-phenyl-2,6,10-triphosphaundecane-P⁽²⁾,P⁽⁶⁾,P⁽¹⁰⁾)nickel(II)

Guidance literature:: In ethanol; addn. of NiBr2*3H2O dissolved in ethanol under vigorous stirring for 2 h; removal of solvent at 20°C/0.1 Torr, residue recrystd. at 20°C from CH2Cl2/ether or 1,2-dichloropropane, elem. anal.;