Borinic acid, cyclohexylmethyl-, methyl ester

Base Information

Chemical Name:Borinic acid, cyclohexylmethyl-, methyl ester
CAS No.:104393-97-7
Molecular Formula:C8H17BO
Molecular Weight:140.033
Hs Code.:

Synonyms:

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Chemical Property of Borinic acid, cyclohexylmethyl-, methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Borinic acid, cyclohexylmethyl-, methyl ester

There total 1 articles about Borinic acid, cyclohexylmethyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: (r)-pinanediol cyclohexylboronate

: 104393-97-7
(C₆H₁₁)B(CH₃)(OCH₃)

: 22422-34-0
(1R,2R,3S,5R)-2,3-pinane diol

Guidance literature:: With hydrogenchloride; methyllithium; In diethyl ether; byproducts: LiCl; stirring of boronate and MeLi in ether (-15°C, 0.5 h), addn. of anhydrous HCl in ether, warming, stirring (25°C, 3 h); evapn., extraction (pentane), treatment with MeOH (25°C, 14 h), drying of pentane phase (MgSO4), solvent removal (vac.); isolation of pinanediol from methanol phase;
DOI:10.1016/0022-328X(88)87067-0

Reference yield:

: 104393-97-7
(C₆H₁₁)B(CH₃)(OCH₃)

: 124-41-4
sodium methylate

: 37981-94-5
dimethyl cyclohexylboronate

Guidance literature:: With iodine; In tetrahydrofuran; methanol; byproducts: MeI; addn. of I2 and NaOMe in MeOH to borinate in THF, stirring (25°C, 14 h); solvent removal (vac.), extraction (pentane), drying (MhSO4), solvent removal (vac.);
DOI:10.1016/0022-328X(88)87067-0