6,7,8,9-Tetrahydro-2-phenylpyrazolo[5,1-c][1,2,4]benzotriazine

Base Information

Chemical Name:6,7,8,9-Tetrahydro-2-phenylpyrazolo[5,1-c][1,2,4]benzotriazine
CAS No.:111005-20-0
Molecular Formula:C₁₅H₁₄N₄
Molecular Weight:250.303
Hs Code.:
DSSTox Substance ID:DTXSID401179640

Synonyms:DTXSID401179640;6,7,8,9-Tetrahydro-2-phenylpyrazolo[5,1-c][1,2,4]benzotriazine;111005-20-0

Suppliers and Price of 6,7,8,9-Tetrahydro-2-phenylpyrazolo[5,1-c][1,2,4]benzotriazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6,7,8,9-Tetrahydro-2-phenylpyrazolo[5,1-c][1,2,4]benzotriazine

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:250.121846464
Heavy Atom Count:19
Complexity:315

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC2=C(C1)N=NC3=CC(=NN23)C4=CC=CC=C4

Technology Process of 6,7,8,9-Tetrahydro-2-phenylpyrazolo[5,1-c][1,2,4]benzotriazine

There total 3 articles about 6,7,8,9-Tetrahydro-2-phenylpyrazolo[5,1-c][1,2,4]benzotriazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1572-10-7
3⁽⁵⁾-phenylpyrazol-5⁽³⁾-amine

: 111005-20-0
2-phenyl-6,7,8,9-tetrahydropyrazolo<5,1-c><1,2,4>triazine

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / HCl, sodium nitrite / H₂O / 15 h / 0 °C

2: 67 percent / 10percent aq. sodium carbonate / CH₂Cl₂ / 0.5 h

3: 12 h / -40 - 10 °C

With hydrogenchloride; sodium carbonate; sodium nitrite; In dichloromethane; water;
DOI:10.1021/jo00234a008

Reference yield:

: 60270-00-0
5-phenyl-3-pyrazolediazonium chloride

: 111005-20-0
2-phenyl-6,7,8,9-tetrahydropyrazolo<5,1-c><1,2,4>triazine

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / 10percent aq. sodium carbonate / CH₂Cl₂ / 0.5 h

2: 12 h / -40 - 10 °C

With sodium carbonate; In dichloromethane;
DOI:10.1021/jo00234a008