2-[2-(diphenylphosphino)ethyl]-6-(9-phenanthryl)pyridinemethylpalladium chloride dimer

Base Information

Chemical Name:2-[2-(diphenylphosphino)ethyl]-6-(9-phenanthryl)pyridinemethylpalladium chloride dimer
CAS No.:1158054-58-0
Molecular Formula:C₆₈H₅₈Cl₂N₂P₂Pd₂
Molecular Weight:1248.92
Hs Code.:

Synonyms:

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Chemical Property of 2-[2-(diphenylphosphino)ethyl]-6-(9-phenanthryl)pyridinemethylpalladium chloride dimer

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Technology Process of 2-[2-(diphenylphosphino)ethyl]-6-(9-phenanthryl)pyridinemethylpalladium chloride dimer

There total 1 articles about 2-[2-(diphenylphosphino)ethyl]-6-(9-phenanthryl)pyridinemethylpalladium chloride dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 1158054-41-1
2-[2-(diphenylphosphanyl)ethyl]-6-(9-phenanthryl)pyridine

: 1158054-58-0
dichloro-μ-(2-[2-(diphenylphosphanyl-1κP)ethyl]-6-(9-phenanthryl)pyridine-2κN)-μ-(2-[2-(diphenylphosphanyl-2κP)ethyl]-6-(9-phenanthryl)pyridine-1κN)(dimethyl)dipalladium

Guidance literature:: In dichloromethane; byproducts: HCl; under N2 using Schlenk techniques; org. ligand (0.43 mmol) and (COD)Pd(CH3)Cl (0.43 mmol) stirred in CH2Cl2 (16 h); concd. (vac.); Et2O added (vigorous stirring); ppt. filtered; washed with Et2O; dried (vac.); elem. anal.;
DOI:10.1002/ejic.200800804

Reference yield: 91.0%

: 1158054-58-0
2-[2-(diphenylphosphino)ethyl]-6-(9-phenanthryl)pyridinemethylpalladium chloride dimer

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 75-05-8,26809-02-9
acetonitrile

: 1158054-70-6
(acetonitrile)(2-[2-(diphenylphosphino)ethyl]-6-(9-phenannthryl)pyridine)methylpalladium tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

Guidance literature:: In acetonitrile; (N2); addn. of CH3CN and CH2Cl2 to 1:1 mixt. of pallladium compd. and borate deriv., stirring for 18 h; cannula filtration, evapn., co-evapn. with pentane, elem. anal.;
DOI:10.1021/om9000378