(4RS,6SR)-4-methyl-2-oxo-6-(2-oxohept-6-enyl)cyclohexanepropanenitrile

Base Information

• Chemical Name: (4RS,6SR)-4-methyl-2-oxo-6-(2-oxohept-6-enyl)cyclohexanepropanenitrile
• CAS No.: 73677-01-7
• Molecular Formula: C₁₇H₂₅NO₂
• Molecular Weight: 275.391
• Mol file: 73677-01-7.mol

Synonyms:

Chemical Property of (4RS,6SR)-4-methyl-2-oxo-6-(2-oxohept-6-enyl)cyclohexanepropanenitrile

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (4RS,6SR)-4-methyl-2-oxo-6-(2-oxohept-6-enyl)cyclohexanepropanenitrile

There total 1 articles about (4RS,6SR)-4-methyl-2-oxo-6-(2-oxohept-6-enyl)cyclohexanepropanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-cyanoethyl)-5-methylcyclohex-2-en-1-one (69060-78-2) + 2-(hept-6-en-2-ylidene)-1,1-dimethylhydrazine (73676-99-0) → (4RS,6SR)-4-methyl-2-oxo-6-(2-oxohept-6-enyl)cyclohexanepropanenitrile (73677-01-7,80471-44-9,80471-45-0)

Guidance literature:

With copper(l) iodide; n-butyllithium; water; thiophenol; Yield given. Multistep reaction; 1.) hexane, THF, -78 deg C, 4 h; -78 deg C to -10 deg C, 2.5 h, 2.) THF, 25 deg C, 16 h;

DOI:10.1021/ja00368a024

upstream raw materials:

2-(2-cyanoethyl)-5-methylcyclohex-2-en-1-one

2-(hept-6-en-2-ylidene)-1,1-dimethylhydrazine

Refernces