(C₅H₅)((CH₃)3CNC)Co(CH(COOCH₃)CH(COOCH₃)C(COOCH₃)C(C₆H₅))

Base Information

Chemical Name:(C₅H₅)((CH₃)3CNC)Co(CH(COOCH₃)CH(COOCH₃)C(COOCH₃)C(C₆H₅))
CAS No.:106800-09-3
Molecular Formula:C₂₆H₃₀CoNO₆
Molecular Weight:511.521
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)((CH<sub>3</sub>)3CNC)Co(CH(COOCH<sub>3</sub>)CH(COOCH<sub>3</sub>)C(COOCH<sub>3</sub>)C(C<sub>6</sub>H<sub>5</sub>))

Synonyms:

Suppliers and Price of (C₅H₅)((CH₃)3CNC)Co(CH(COOCH₃)CH(COOCH₃)C(COOCH₃)C(C₆H₅))

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (C₅H₅)((CH₃)3CNC)Co(CH(COOCH₃)CH(COOCH₃)C(COOCH₃)C(C₆H₅))

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (C₅H₅)((CH₃)3CNC)Co(CH(COOCH₃)CH(COOCH₃)C(COOCH₃)C(C₆H₅))

There total 3 articles about (C₅H₅)((CH₃)3CNC)Co(CH(COOCH₃)CH(COOCH₃)C(COOCH₃)C(C₆H₅)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 53559-30-1
(η5-C5H5)Co{C(C6H5)=C(CO2CH3)CH(CO2CH3)CH(-cyclo-Co)(CO2CH3)}{P(C6H5)3}

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 106800-09-3
(η5-C5H5)Co{C(C6H5)=C(CO2CH3)CH(CO2CH3)CH(-cyclo-Co)(CO2CH3)}{CNC(CH3)3}*1/3H2O

Guidance literature:: In benzene; heated in a 50°C oil bath for 5 h under nitrogen atmosphere; concd., chromd. on a SiO2 column (eluent benzene-THF), recrystd. from benzene-hexane;
DOI:10.1021/om00147a015

Reference yield: 76.0%

: 113158-74-0
(η5-cyclopentadienyl)cobalt{(phenyl)(dicarbomethoxy)(OCH3)-oxanorbornadiene}

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 106800-09-3
(C₅H₅)((CH₃)3CNC)Co(CH(COOCH₃)CH(COOCH₃)C(COOCH₃)C(C₆H₅))

: 110170-95-1
(C₅H₅)((CH₃)3CNC)Co(CH(COOCH₃)CH(COOCH₃)C(COOCH₃)C(C₆H₅))

Guidance literature:: In benzene; soln. of Co-complex and an excess of t-BuNC in benzene was allowed to stirr for 3 h under inert atmosphere; evapd., residue was chromd. on a silica column (eluent CH2Cl2-THF), major isomer was recrystd. from toluene-hexane;
DOI:10.1021/om00153a031

Reference yield: 68.0%

: 113158-74-0
(η5-cyclopentadienyl)cobalt{(phenyl)(dicarbomethoxy)(OCH3)-oxanorbornadiene}

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 106800-09-3
(η5-C5H5)Co{C(C6H5)=C(CO2CH3)CH(CO2CH3)CH(-cyclo-Co)(CO2CH3)}{CNC(CH3)3}*1/3H2O

Guidance literature:: In benzene; stirred at room temp. for 45 min under nitrogen atmosphere; concd., addn. of hexane afforded crystals of the product; elem. anal., water by Karl Fisher titrn.;
DOI:10.1021/om00147a015