Benzeneethanamine, 3,4-dimethoxy-2-(methylthio)-

Base Information

Chemical Name:Benzeneethanamine, 3,4-dimethoxy-2-(methylthio)-
CAS No.:75510-74-6
Molecular Formula:C₁₁H₁₇NO₂S
Molecular Weight:227.327
Hs Code.:
UNII:L9542D99QQ
ChEMBL ID:CHEMBL281325

Synonyms:2-Tim;Benzeneethanamine, 3,4-dimethoxy-2-(methylthio)-;L9542D99QQ;2-Thioxy-3,4-methoxy-phenethylamine;75510-74-6;2-(3,4-dimethoxy-2-(methylthio)phenyl)ethanamine;UNII-L9542D99QQ;3,4-Dimethoxy-2-(methylthio)benzeneethanamine;2-(3,4-Dimethoxy-2-(methylsulfanyl)phenyl)ethan-1-amine;CHEMBL281325;SCHEMBL11460791

Suppliers and Price of Benzeneethanamine, 3,4-dimethoxy-2-(methylthio)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzeneethanamine, 3,4-dimethoxy-2-(methylthio)-

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:227.09799996
Heavy Atom Count:15
Complexity:180

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)CCN)SC)OC

Technology Process of Benzeneethanamine, 3,4-dimethoxy-2-(methylthio)-

There total 3 articles about Benzeneethanamine, 3,4-dimethoxy-2-(methylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78335-81-6
2-(methylthio)-3,4-dimethoxy-β-nitrostyrene

: 75510-74-6
2-(2-Methylthio-3,4-dimethoxyphenyl)-ethylamine

Guidance literature:: With lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran; for 0.0833333h; Heating;
DOI:10.1021/jm00143a017

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 75510-74-6
2-(2-Methylthio-3,4-dimethoxyphenyl)-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / n-butyllithium, TMEDA / hexane; petroleum ether / 0.5 h

2: 1.) POCl₃, 2.) ammonium acetate / 1.) reflux, 2.5 h, 2.) reflux, 5 h

3: LiAlH₄, H₂SO₄ / tetrahydrofuran / 0.08 h / Heating

With ammonium acetate; lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; trichlorophosphate; In tetrahydrofuran; hexane; Petroleum ether;
DOI:10.1021/jm00143a017

Reference yield:

: 51506-47-9
2,3-dimethoxythioanisole

: 75510-74-6
2-(2-Methylthio-3,4-dimethoxyphenyl)-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) POCl₃, 2.) ammonium acetate / 1.) reflux, 2.5 h, 2.) reflux, 5 h

2: LiAlH₄, H₂SO₄ / tetrahydrofuran / 0.08 h / Heating

With ammonium acetate; lithium aluminium tetrahydride; sulfuric acid; trichlorophosphate; In tetrahydrofuran;
DOI:10.1021/jm00143a017