[1-CH₂Cy-closo-C₂B₁₀H₁₁]

Base Information

Chemical Name:[1-CH₂Cy-closo-C₂B₁₀H₁₁]
CAS No.:934008-26-1
Molecular Formula:C₉H₂₄B₁₀
Molecular Weight:240.4
Hs Code.:

[1-CH<sub>2</sub>Cy-closo-C<sub>2</sub>B<sub>10</sub>H<sub>11</sub>]

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Chemical Property of [1-CH₂Cy-closo-C₂B₁₀H₁₁]

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Technology Process of [1-CH₂Cy-closo-C₂B₁₀H₁₁]

There total 1 articles about [1-CH₂Cy-closo-C₂B₁₀H₁₁] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 17702-41-9
nido-decaborane

: 17715-00-3
prop-2-ynylcyclohexane

: 934008-26-1
[1-CH₂Cy-closo-C₂B₁₀H₁₁]

Guidance literature:: In toluene; acetonitrile; under N2 atm. soln. decaborane in MeCN-toluene was refluxed for 1 h, 3-cyclohexyl-1-propyne was added and refluxed for 15 h; solvent was removed in vacuo, chromy. on silica (10 % CH2Cl2 in hexane);
DOI:10.1021/ic0617543

Reference yield: 70.0%

: 7789-23-3
potassium fluoride

: [Re(carbonyl)3(water)3]Br

: 934008-26-1
[1-CH₂Cy-closo-C₂B₁₀H₁₁]

: [K][3,3,3-(CO)3-1-CH₂Cy)-closo-ReC₂B₉H₁o]

Guidance literature:: In ethanol; water; other Radiation; closo-carborane, KF, and (Re(CO)3(H2O)3)Br in aq. EtOH was heated at 200°C for 15 min in microwave reactor, additional portion Re complexwas added and heated at 200°C for 10 min; solvent was evapd. to dryness under N2 stream, chromy. on silica using automated purification system (3-30 % MeOH in CH2Cl2);
DOI:10.1021/ic0617543