C₅₀H₅₆N₇O₇P

Base Information

Chemical Name:C₅₀H₅₆N₇O₇P
CAS No.:1092804-06-2
Molecular Formula:C₅₀H₅₆N₇O₇P
Molecular Weight:898.011
Hs Code.:

C<sub>50</sub>H<sub>56</sub>N<sub>7</sub>O<sub>7</sub>P

Synonyms:

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Chemical Property of C₅₀H₅₆N₇O₇P

Chemical Property:

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Technology Process of C₅₀H₅₆N₇O₇P

There total 13 articles about C₅₀H₅₆N₇O₇P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1092804-05-1
C₂₀H₂₁N₅O₄

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 102691-36-1
N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

: 1092804-06-2
C₅₀H₅₆N₇O₇P

Guidance literature:: C₂₀H₂₁N₅O₄; 4,4'-dimethoxytrityl chloride;

N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite; With 1-methyl-1H-imidazole; 1H-tetrazole;

Reference yield:

: 956485-06-6
3-O-(2-naphthylmethyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 1092804-06-2
C₅₀H₅₆N₇O₇P

Guidance literature:: Multi-step reaction with 14 steps

1.1: water; acetic acid / 16 h / 20 °C

2.1: sodium periodate / 1,4-dioxane; water / 1.67 h

3.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

4.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

6.2: 16.33 h / -78 - 20 °C

7.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

7.2: 4 h / 50 °C

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

8.2: 0.5 h

9.1: n-butyllithium / tetrahydrofuran; hexanes / 2 h / 0 °C

9.2: 16 h / -78 - 20 °C

10.1: acetic anhydride; sulfuric acid; acetic acid

10.2: Reflux

11.1: dmap

12.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride

13.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone

With dmap; sodium periodate; n-butyllithium; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); sulfuric acid; water; tri-n-butyl-tin hydride; acetic anhydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; 10.2: Vorbrugen Reaction;

Reference yield:

: 1057385-93-9
(3aR,5S,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxole-5-carbaldehyde

: 1092804-06-2
C₅₀H₅₆N₇O₇P

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

2.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

4.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

4.2: 16.33 h / -78 - 20 °C

5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

5.2: 4 h / 50 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 0.5 h

7.1: n-butyllithium / tetrahydrofuran; hexanes / 2 h / 0 °C

7.2: 16 h / -78 - 20 °C

8.1: acetic anhydride; sulfuric acid; acetic acid

8.2: Reflux

9.1: dmap

10.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride

11.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone

With dmap; n-butyllithium; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); sulfuric acid; tri-n-butyl-tin hydride; acetic anhydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; methanol; hexanes; dichloromethane; water; 8.2: Vorbrugen Reaction;