C₁₃H₁₅Cl₃N₂O₄S

Base Information

• Chemical Name: C₁₃H₁₅Cl₃N₂O₄S
• CAS No.: 1354438-39-3
• Molecular Formula: C₁₃H₁₅Cl₃N₂O₄S
• Molecular Weight: 401.698
• Mol file: 1354438-39-3.mol

Synonyms:

Chemical Property of C₁₃H₁₅Cl₃N₂O₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₃H₁₅Cl₃N₂O₄S

There total 4 articles about C₁₃H₁₅Cl₃N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H9Cl3N2O2S (1354438-29-1) + ethyl bromoacetate (105-36-2) → C13H15Cl3N2O4S (1354438-39-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

DOI:10.1021/ml200226x

Reference yield:

C9H10Cl4N2O2S (1354438-24-6) → C13H15Cl3N2O4S (1354438-39-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / dimethyl sulfoxide / 2 h / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

With potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1021/ml200226x

Reference yield:

2,4,6-trichloroaniline (634-93-5) → C13H15Cl3N2O4S (1354438-39-3)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / diethyl ether / 4 h

2: potassium carbonate / dimethyl sulfoxide / 2 h / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

With potassium carbonate; triethylamine; In diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1021/ml200226x

upstream raw materials:

C₉H₁₀Cl₄N₂O₂S

C₉H₉Cl₃N₂O₂S

ethyl bromoacetate

2,4,6-trichloroaniline

Downstream raw materials:

C₁₁H₁₁Cl₃N₂O₄S