Diphenyl pyridine-2,6-dicarboxylate

Base Information

Chemical Name:Diphenyl pyridine-2,6-dicarboxylate
CAS No.:10448-12-1
Molecular Formula:C19H13NO4
Molecular Weight:319.317
Hs Code.:
DSSTox Substance ID:DTXSID90361177
Nikkaji Number:J803.111H
Wikidata:Q82143377
Mol file:10448-12-1.mol

Synonyms:diphenyl pyridine-2,6-dicarboxylate;10448-12-1;SCHEMBL69458;DTXSID90361177;2,6-Pyridinedicarboxylic acid diphenyl ester;AN-652/04425050

Suppliers and Price of Diphenyl pyridine-2,6-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diphenyl pyridine-2,6-dicarboxylate

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:319.08445790
Heavy Atom Count:24
Complexity:389

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)OC(=O)C2=NC(=CC=C2)C(=O)OC3=CC=CC=C3

Technology Process of Diphenyl pyridine-2,6-dicarboxylate

There total 4 articles about Diphenyl pyridine-2,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 626-05-1
2,6-Dibromopyridine

: 1864-94-4
phenyl formate

: 10448-12-1
2,6-pyridinedicarboxylic acid diphenyl ester

Guidance literature:: With palladium diacetate; triethylamine; tri tert-butylphosphoniumtetrafluoroborate; In acetonitrile; at 80 ℃; Inert atmosphere;
DOI:10.1021/ol301192s

Reference yield:

: 108-95-2,27073-41-2
phenol

: 10448-12-1
2,6-pyridinedicarboxylic acid diphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 1 h / 60 °C / Inert atmosphere

1.2: 2.5 h / Inert atmosphere

2.1: palladium diacetate; triethylamine; tri tert-butylphosphoniumtetrafluoroborate / acetonitrile / 80 °C / Inert atmosphere

With palladium diacetate; acetic anhydride; triethylamine; tri tert-butylphosphoniumtetrafluoroborate; In acetonitrile;
DOI:10.1021/ol301192s