C₆H₅P(CH₂CH₂S)2Sn

Base Information

Chemical Name:C₆H₅P(CH₂CH₂S)2Sn
CAS No.:78610-88-5
Molecular Formula:C₁₀H₁₃PS₂Sn
Molecular Weight:347.029
Hs Code.:

C<sub>6</sub>H<sub>5</sub>P(CH<sub>2</sub>CH<sub>2</sub>S)2Sn

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆H₅P(CH₂CH₂S)2Sn

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Technology Process of C₆H₅P(CH₂CH₂S)2Sn

There total 1 articles about C₆H₅P(CH₂CH₂S)2Sn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 3190-78-1
3-phenyl-3-phosphapentane-1,5-dithiol

: 14254-05-8,26306-46-7,130287-64-8
tin(II) n-butoxide

: 78610-88-5,102503-25-3
C₆H₅P(CH₂CH₂S)2Sn

Guidance literature:: In toluene; byproducts: n-butanol; dropwise addn. of a soln. of C6H5P(CH2CH2SH)2 in toluene to a vigorously stirred soln. of Sn(OC4H9)2 in toluene; 2 h at 40°C; performed under dry argon;; removal of solvent; recrystn. from benzene; elem. anal.;;
DOI:10.1016/S0022-328X(00)99679-7

Reference yield: 78.6%

: 78610-88-5,102503-25-3
C₆H₅P(CH₂CH₂S)2Sn

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 107936-85-6
pentacarbonyl-5-phenyl-5-phospha-2,8-dithia-1-stannabicyclo{3.3.0(1.5)}octanechromium⁽⁰⁾

Guidance literature:: With THF; In tetrahydrofuran; byproducts: CO; Irradiation (UV/VIS); Sn(SCH2CH2)2PC6H5 and Cr(CO)5(THF), generated from Cr(CO)6 by UV-irradiation, was stirred for 5 h in THF; performed under dry argon;; removal of solvent in vac.; the residue was kept at 0.2 mmHg; recrystn.from benzene; elem. anal.;;
DOI:10.1016/S0022-328X(00)99679-7