(5S,6S,10R)-10-(2-bromophenyl)-14-[(E)-1-(2-bromophenyl)methylidene]-3,9-di(4-chlorophenyl)-12-(1-phenylethyl)-1,4,7-trioxa-2,8,12-triazadispiro[4.0.4.4]-tetradeca-2,8-diene

Base Information

• Chemical Name: (5S,6S,10R)-10-(2-bromophenyl)-14-[(E)-1-(2-bromophenyl)methylidene]-3,9-di(4-chlorophenyl)-12-(1-phenylethyl)-1,4,7-trioxa-2,8,12-triazadispiro[4.0.4.4]-tetradeca-2,8-diene
• CAS No.: 1245653-74-0
• Molecular Formula: C₄₁H₃₁Br₂Cl₂N₃O₃
• Molecular Weight: 844.429

Synonyms:

Chemical Property of (5S,6S,10R)-10-(2-bromophenyl)-14-[(E)-1-(2-bromophenyl)methylidene]-3,9-di(4-chlorophenyl)-12-(1-phenylethyl)-1,4,7-trioxa-2,8,12-triazadispiro[4.0.4.4]-tetradeca-2,8-diene

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Technology Process of (5S,6S,10R)-10-(2-bromophenyl)-14-[(E)-1-(2-bromophenyl)methylidene]-3,9-di(4-chlorophenyl)-12-(1-phenylethyl)-1,4,7-trioxa-2,8,12-triazadispiro[4.0.4.4]-tetradeca-2,8-diene

There total 1 articles about (5S,6S,10R)-10-(2-bromophenyl)-14-[(E)-1-(2-bromophenyl)methylidene]-3,9-di(4-chlorophenyl)-12-(1-phenylethyl)-1,4,7-trioxa-2,8,12-triazadispiro[4.0.4.4]-tetradeca-2,8-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

3,5-bis[(E)-(2-bromophenyl)methylidene]-1-[(R)-1-phenylethyl]tetrahydro-4(1H)-pyridinone (1245653-62-6) + 4-chlorobenzohydroximoyl chloride (28123-63-9) → 4,11-bis(2-bromophenyl)-3,10-bis(4-chlorophenyl)-13-((R)-1-phenylethyl)-1,8-dioxa-2,9,13-triazadispiro[4.1.4.3]tetradeca-2,9-dien-6-one (1245740-91-3) + (5R,6R,10S)-10-(2-bromophenyl)-14-[(E)-1-(2-bromophenyl)methylidene]-3,9-di(4-chlorophenyl)-12-(1-phenylethyl)-1,4,7-trioxa-2,8,12-triazadispiro[4.0.4.4]-tetradeca-2,8-diene (1245653-90-0) + (5S,6S,10R)-10-(2-bromophenyl)-14-[(E)-1-(2-bromophenyl)methylidene]-3,9-di(4-chlorophenyl)-12-(1-phenylethyl)-1,4,7-trioxa-2,8,12-triazadispiro[4.0.4.4]-tetradeca-2,8-diene (1245653-74-0) + (4R,5S,6R,11R,15S)-4,15-bis(2-bromophenyl)-3,9,14-tri(4-chlorophenyl)-17-(1-phenylethyl)-1,7,10,12-tetraoxa-2,8,13,17-tetraazatrispiro[4.0.4.0.4.3]octadeca-2,8,13-triene (1245654-00-5)

Guidance literature:

With triethylamine; In benzene; at 20 ℃; diastereoselective reaction;

DOI:10.1016/j.tetasy.2010.03.054

upstream raw materials:

3,5-bis[(E)-(2-bromophenyl)methylidene]-1-[(R)-1-phenylethyl]tetrahydro-4(1H)-pyridinone

4-chlorobenzohydroximoyl chloride

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