5-Diethylamino-4-methyl-1-1,N¹-dimethyl-N²-(4-nitrophenylsulfonyl)amidino>-1,2,3-triazol

Base Information

• Chemical Name: 5-Diethylamino-4-methyl-1-1,N¹-dimethyl-N²-(4-nitrophenylsulfonyl)amidino>-1,2,3-triazol
• CAS No.: 84275-01-4
• Molecular Formula: C₁₆H₂₃N₇O₄S
• Molecular Weight: 409.469

Synonyms:

Chemical Property of 5-Diethylamino-4-methyl-1-1,N¹-dimethyl-N²-(4-nitrophenylsulfonyl)amidino>-1,2,3-triazol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 5-Diethylamino-4-methyl-1-1,N¹-dimethyl-N²-(4-nitrophenylsulfonyl)amidino>-1,2,3-triazol

There total 3 articles about 5-Diethylamino-4-methyl-1-1,N¹-dimethyl-N²-(4-nitrophenylsulfonyl)amidino>-1,2,3-triazol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

N--4-nitrobenzolsulfonamid (84274-78-2) + methyl(diethylamino)acetylene (4231-35-0) → 5-Diethylamino-4-methyl-1-1,N1-dimethyl-N2-(4-nitrophenylsulfonyl)amidino>-1,2,3-triazol (84275-01-4)

Guidance literature:

In chloroform; for 48h; Ambient temperature;

Reference yield:

p-nitrobenzenesulfonamide (6325-93-5) → 5-Diethylamino-4-methyl-1-1,N1-dimethyl-N2-(4-nitrophenylsulfonyl)amidino>-1,2,3-triazol (84275-01-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / benzene / 2 h / Heating

2: 76 percent / NaN₃ / acetone; H₂O / 1.) 1h, 0 degC, 2.) 1h, room temp.

3: 73 percent / CHCl₃ / 48 h / Ambient temperature

With sodium azide; In chloroform; water; acetone; benzene;

Reference yield:

N--4-nitrobenzolsulfonamid (40676-68-4) → 5-Diethylamino-4-methyl-1-1,N1-dimethyl-N2-(4-nitrophenylsulfonyl)amidino>-1,2,3-triazol (84275-01-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / NaN₃ / acetone; H₂O / 1.) 1h, 0 degC, 2.) 1h, room temp.

2: 73 percent / CHCl₃ / 48 h / Ambient temperature

With sodium azide; In chloroform; water; acetone;

upstream raw materials:

N--4-nitrobenzolsulfonamid

methyl(diethylamino)acetylene

p-nitrobenzenesulfonamide

N--4-nitrobenzolsulfonamid

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