C₇₄H₇₅Cl₃N₂O₁₈

Base Information

• Chemical Name: C₇₄H₇₅Cl₃N₂O₁₈
• CAS No.: 118590-80-0
• Molecular Formula: C₇₄H₇₅Cl₃N₂O₁₈
• Molecular Weight: 1386.77
• Mol file: 118590-80-0.mol

Synonyms:

Chemical Property of C₇₄H₇₅Cl₃N₂O₁₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₇₄H₇₅Cl₃N₂O₁₈

There total 6 articles about C₇₄H₇₅Cl₃N₂O₁₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) → C74H75Cl3N2O18 (118590-80-0)

Guidance literature:

Multi-step reaction with 5 steps

1: Ag₂O-KI / dimethylformamide

2: TFA,H₂O,THF

3: DMAP / pyridine

4: PdCl₂-AcONa / aq. acetic acid

5: DBU / 1,2-dichloro-ethane

With dmap; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; palladium dichloride; silver(l) oxide; In pyridine; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)80733-9

Reference yield:

C71H75NO16 (118590-78-6) → C74H75Cl3N2O18 (118590-80-0)

Guidance literature:

Multi-step reaction with 3 steps

1: DMAP / pyridine

2: PdCl₂-AcONa / aq. acetic acid

3: DBU / 1,2-dichloro-ethane

With dmap; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; In pyridine; acetic acid; 1,2-dichloro-ethane;

DOI:10.1016/S0040-4039(00)80733-9

Reference yield:

C74H79NO16 (118590-76-4) → C74H75Cl3N2O18 (118590-80-0)

Guidance literature:

Multi-step reaction with 4 steps

1: TFA,H₂O,THF

2: DMAP / pyridine

3: PdCl₂-AcONa / aq. acetic acid

4: DBU / 1,2-dichloro-ethane

With dmap; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; palladium dichloride; In pyridine; acetic acid; 1,2-dichloro-ethane;

DOI:10.1016/S0040-4039(00)80733-9

upstream raw materials:

C₇₂H₇₅NO₁₈

trichloroacetonitrile

benzyl bromide

C₆₀H₆₇NO₁₆

Downstream raw materials:

C₁₃₁H₁₃₉NO₂₉

C₇₂H₇₃NO₁₇

C₁₃₃H₁₃₇NO₂₈