1,3,4,5-tetramethylimidazol-2-ylidene tetraphenoxyaluminate

Base Information

Chemical Name:1,3,4,5-tetramethylimidazol-2-ylidene tetraphenoxyaluminate
CAS No.:835875-23-5
Molecular Formula:C₇H₁₃N₂*C₂₄H₂₀AlO₄
Molecular Weight:524.596
Hs Code.:

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Chemical Property of 1,3,4,5-tetramethylimidazol-2-ylidene tetraphenoxyaluminate

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Technology Process of 1,3,4,5-tetramethylimidazol-2-ylidene tetraphenoxyaluminate

There total 1 articles about 1,3,4,5-tetramethylimidazol-2-ylidene tetraphenoxyaluminate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 835875-22-4
(1,3,4,5-tetramethylimidazolin-2-ylidene)*AlH₃

: 108-95-2,27073-41-2
phenol

: 835875-23-5
1,3,4,5-tetramethylimidazol-2-ylidene tetraphenoxyaluminate

Guidance literature:: In tetrahydrofuran; diethyl ether; At atm.; phenol in diethyl ether was added dropwise to AlH3-complex in THF at -50°C, warmed to ambient temp., stirred for 2 h; volatiles were removed in vac.; extd. into fresh THF followed by placement at -35°C overnight;
DOI:10.1016/j.ica.2004.07.036