(CH₃)3PBH₂P(C₆H₅)2BH₂OSO₂CH₃

Base Information

• Chemical Name: (CH₃)3PBH₂P(C₆H₅)2BH₂OSO₂CH₃
• CAS No.: 122953-48-4
• Molecular Formula: C₁₆H₂₆B₂O₃P₂S
• Molecular Weight: 382.016
• Mol file: 122953-48-4.mol

Synonyms:

Chemical Property of (CH₃)3PBH₂P(C₆H₅)2BH₂OSO₂CH₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (CH₃)3PBH₂P(C₆H₅)2BH₂OSO₂CH₃

There total 1 articles about (CH₃)3PBH₂P(C₆H₅)2BH₂OSO₂CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methanesulfonic acid (75-75-2,98527-29-8) + (CH3)3PBH2P(C6H5)2BH3 (122971-97-5) → (CH3)3PBH2P(C6H5)2BH2OSO2CH3 (122953-48-4)

Guidance literature:

With potassium hydrogencarbonate; In dichloromethane; MeOSO3 added to a soln. of the borane, KHCO3 added, stirring, mixture passed through a column (silica gel, ethylacetate; concg. (vac.), elem. anal.;

DOI:10.1246/bcsj.63.2846

Reference yield: 79.0%

(CH3)3PBH2P(C6H5)2BH2OSO2CH3 (122953-48-4) + diphenylphosphineborane (41593-58-2) → (CH3)3PBH2P(C6H5)2BH2P(C6H5)2BH3 (122953-49-5)

Guidance literature:

With sodium hydride; In tetrahydrofuran; reactants added to a NaH suspn. (0°C), stirring (room temp.), quenching (HCl); extn. (CHCl3), washing (brine), drying (MgSO4), chromatography (silica gel, AcOEt/hexane, pasty mass triturated (ether), elem. anal.;

DOI:10.1246/bcsj.63.2846

upstream raw materials:

methanesulfonic acid

(CH₃)3PBH₂P(C₆H₅)2BH₃

Downstream raw materials:

(CH₃)3PBH₂P(C₆H₅)2BH₂P(C₆H₅)2BH₃

Refernces