trans-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline

Base Information

• Chemical Name: trans-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline
• CAS No.: 114916-44-8
• Molecular Formula: C₂₁H₂₅NO
• Molecular Weight: 307.436

Synonyms:

Chemical Property of trans-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline

There total 1 articles about trans-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

benzyl chloride (100-44-7) + 9-Methoxy-1,2,3,4,4a,5,10,10a-octahydro-benzo[g]quinoline (340966-75-8) → cis-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline (114916-44-8,114916-45-9,131380-24-0,131483-93-7,131484-04-3,131484-05-4,131484-06-5) + trans-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline hydrochloride (114916-46-0,114916-47-1,131380-27-3,131563-43-4,131563-44-5)

Guidance literature:

With potassium carbonate; In acetonitrile; Ambient temperature;

DOI:10.1016/S0040-4020(01)87725-5

Reference yield: 69.0%

cis-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline (114916-44-8,114916-45-9,131380-24-0,131483-93-7,131484-04-3,131484-05-4,131484-06-5) → (+)-(4aS,10aR)-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline (131483-93-7)

Guidance literature:

DOI:10.1021/jm00106a004

Reference yield: 63.0%

cis-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline (114916-44-8,114916-45-9,131380-24-0,131483-93-7,131484-04-3,131484-05-4,131484-06-5) → (-)-(4aR,10aS)-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline (131484-04-3)

Guidance literature:

DOI:10.1021/jm00106a004

upstream raw materials:

benzyl chloride

9-Methoxy-1,2,3,4,4a,5,10,10a-octahydro-benzo[g]quinoline

Downstream raw materials:

(-)-(4aR,10aS)-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline

(+)-(4aS,10aR)-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline

(+)-(4aS,10aS)-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline hydrochloride

(-)-(4aR,10aR)-1-benzyl-1,2,3,4,4a,5,10,10a-octahydro-9-methoxybenzoquinoline hydrochloride

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