meso-1,3,4,6-tetrakis(3-formylphenyl)-1,5-hexadiene

Base Information

Chemical Name:meso-1,3,4,6-tetrakis(3-formylphenyl)-1,5-hexadiene
CAS No.:103954-02-5
Molecular Formula:C₃₄H₂₆O₄
Molecular Weight:498.578
Hs Code.:

Synonyms:

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Chemical Property of meso-1,3,4,6-tetrakis(3-formylphenyl)-1,5-hexadiene

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Technology Process of meso-1,3,4,6-tetrakis(3-formylphenyl)-1,5-hexadiene

There total 12 articles about meso-1,3,4,6-tetrakis(3-formylphenyl)-1,5-hexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3132-99-8
m-bromobenzoic aldehyde

: 103954-02-5
meso-1,3,4,6-tetrakis(3-formylphenyl)-1,5-hexadiene

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / NaOH / ethanol; methanol

2: 98 percent / NaBH₄ / methanol / 1 h

3: 90 percent / acetic acid, HBr / 12 h / 0 °C

4: Fe / dimethylformamide / 60 °C

5: 1.) n-BuLi / 1.) hexane, 2 h, 2.) hexane 2 h

With sodium hydroxide; sodium tetrahydroborate; n-butyllithium; hydrogen bromide; iron; acetic acid; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00234a010

Reference yield:

: 103953-98-6
1,3-bis-(3-bromophenyl)-2-propen-1-ene

: 103954-02-5
meso-1,3,4,6-tetrakis(3-formylphenyl)-1,5-hexadiene

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / NaBH₄ / methanol / 1 h

2: 90 percent / acetic acid, HBr / 12 h / 0 °C

3: Fe / dimethylformamide / 60 °C

4: 1.) n-BuLi / 1.) hexane, 2 h, 2.) hexane 2 h

With sodium tetrahydroborate; n-butyllithium; hydrogen bromide; iron; acetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00234a010

Reference yield:

: 103953-99-7
1,3-bis-(3-bromophenyl)-1-hydroxy-2-propene

: 103954-02-5
meso-1,3,4,6-tetrakis(3-formylphenyl)-1,5-hexadiene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / acetic acid, HBr / 12 h / 0 °C

2: Fe / dimethylformamide / 60 °C

3: 1.) n-BuLi / 1.) hexane, 2 h, 2.) hexane 2 h

With n-butyllithium; hydrogen bromide; iron; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jo00234a010