C₃₂H₃₄N₄O₆

Base Information

• Chemical Name: C₃₂H₃₄N₄O₆
• CAS No.: 1443775-99-2
• Molecular Formula: C₃₂H₃₄N₄O₆
• Molecular Weight: 570.645
• Mol file: 1443775-99-2.mol

Synonyms:

Chemical Property of C₃₂H₃₄N₄O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₃₄N₄O₆

There total 3 articles about C₃₂H₃₄N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

ethyl 4-(benzoylamino)pyrrole-2-carboxylate + butyraldehyde (123-72-8) → C32H34N4O6 (1443775-99-2)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane;

DOI:10.1055/s-0032-1318503

Reference yield:

Ethyl 4-nitropyrrole-2-carboxylate (5930-92-7) → C32H34N4O6 (1443775-99-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 5%-palladium/activated carbon; hydrogen / methanol / 16 h

2: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Cooling with ice

3: toluene-4-sulfonic acid / dichloromethane

With 5%-palladium/activated carbon; hydrogen; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane;

DOI:10.1055/s-0032-1318503

Reference yield:

4-amino-2-ethoxycarbonyl-pyrrole (67318-12-1) → C32H34N4O6 (1443775-99-2)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 16 h / 0 - 20 °C / Cooling with ice

2: toluene-4-sulfonic acid / dichloromethane

With toluene-4-sulfonic acid; triethylamine; In dichloromethane;

DOI:10.1055/s-0032-1318503

upstream raw materials:

Ethyl 4-nitropyrrole-2-carboxylate

4-amino-2-ethoxycarbonyl-pyrrole

butyraldehyde

Refernces